Crystallization Process Systems 1st Edition by Jones 0750655208 9780750655200

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ISBN 10: 0750655208

ISBN 13: 9780750655200

Author: A. G. Jones

Crystallization Process Systems gives a clear, concise, balanced and up to date presentation of crystallization and solid-liquid separation of the crystalline product. The information is presented in a coherent, concise and logical sequence based on the fundamentals of particulate crystallization processes as systems.

By emphasising the analysis, design and operation of particulate crystallization processes as systems, the reader will be able to make a better judgement about the best, cheapest and most effective production method to use.

Presents a coherent, concise and logical sequence based on the fundamentals of particulate crystallization processes as systemsEmphasis on the design and optimization of the crystallization processing system

Crystallization Process Systems 1st Table of contents:

Chapter 1. Particulate crystal characteristics

Crystal characteristics

Single particles

Particle size distributions

Packing characteristics

Techniques for particle sizing and characterization

Chapter 2. Fluid-particle transport processes

Particle-fluid hydrodynamics

Sedimentation

Slurries

Fluid flow through porous media

Suspension of settling particles by agitation

Mixing models

The population balance

Chapter 3. Crystallization principles and techniques

Phase equilibria

Types of crystallizer

The mixed suspension, mixed product removal (MSMPR) crystallizer

Population balance

Precipitation

Chapter 4. Solid-liquid separation processes

Settling tanks

Thickeners

Filters and filtration

Types of filter

Theory of filtration

Leaf test

Optimum cycle time during batch filtration

Continuous rotary vacuum filtration

Centrifuges

Solid bowl centrifuge

Thin layer solid bowl centrifuge

Centrifugal filtration

Hydrocyclones

Crystal washing

Crystal drying

Chapter 5. Crystal formation and breakage

Crystallization and precipitation kinetics

Nucleation

Crystal growth

Induction periods

Determination of crystal growth and nucleation kinetics

Particle breakage processes

Secondary nucleation

Chapter 6. Crystal agglomeration and disruption

Agglomerate particle form

Colloid and surface science

Population balance

Agglomeration and disruption during precipitation

Determination of precipitation kinetics

Troubleshooting agglomeration

Chapter 7. Crystallizer design and performance

Design and performance of batch crystallizers

Batch crystallizer design and operation

Prediction of CSD

Programmed cooling crystallization

Design and performance of continuous crystallizers

Chapter 8. Crystallizer mixing and scale-up

Liquid-liquid crystallization systems

Gas-liquid crystal precipitation

Microcrystallizers

Chapter 9. Design of crystallization process systems

Crystallization process systems design

Crystallization process models

Crystallization process synthesis

Crystallization process systems simulation

Crystallization process instrumentation and control

Crystallization in practice

References

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