Crystallization 4th Edition by Mullin 0750648333 9780750648332
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Authors:J W Mullin , Series:Medical [23] , Tags:Science; Physics; Crystallography; Chemistry; Industrial & Technical; Applied Sciences; Technology & Engineering; Chemical & Biochemical , Author sort:Mullin, J W , Ids:9780080530116 , Languages:Languages:eng , Published:Published:May 2001 , Publisher:Elsevier , Comments:Comments:Since the first publication of this definitive work nearly 40 years ago, this fourth edition has been completely rewritten. Crystallization is used at some stage in nearly all process industries as a method of production, purification or recovery of solid materials. Incorporating all the recent developments and applications of crystallization technology, Crystallization gives clear accounts of the underlying principles, a review of the past and current research themes and guidelines for equipment and process design. This new edition introduces and enlarges upon such subjects as: Control and Separation of polymorphs and chiral crystals Micro- and macro-mixing and the use of computer fluid dynamics Seeding and secondary nucleation in batch crystallization processes Incorporation of upstream and downstream requirements into design procedures for crystallization plant Computer-aided molecular design and its use in crystal habit modifier selection Crystallization provides a comprehensive overview of the subject and will prove invaluable to all chemical engineers and industrial chemists in the process industries as well as crystallization workers and students in industry and academia. Crystallization is written with the precision and clarity of style that is John Mullin’s hallmark – a special feature being the large number of appendices that provide relevant physical property data. Covers all new developments and trends in crystallization Comprehensive coverage of subject area
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ISBN 10: 0750648333
ISBN 13: 9780750648332
Author: J W Mullin
Crystallization is used at some stage in nearly all process industries as a method of production, purification or recovery of solid materials.
Incorporating all the recent developments and applications of crystallization technology, Crystallization gives clear accounts of the underlying principles, a review of the past and current research themes and guidelines for equipment and process design. This new edition introduces and enlarges upon such subjects as:
· Control and Separation of polymorphs and chiral crystals
· Micro- and macro-mixing and the use of computer fluid dynamics
· Seeding and secondary nucleation in batch crystallization processes
· Incorporation of upstream and downstream requirements into design procedures for crystallization plant
· Computer-aided molecular design and its use in crystal habit modifier selection
Crystallization provides a comprehensive overview of the subject and will prove invaluable to all chemical engineers and industrial chemists in the process industries as well as crystallization workers and students in industry and academia.
Crystallization is written with the precision and clarity of style that is John Mullin’s hallmark – a special feature being the large number of appendices that provide relevant physical property data.
Covers all new developments and trends in crystallization.
Comprehensive coverage of subject area.
Crystallization 4th Table of contents:
Chapter 1. The crystalline state
1.1 Liquid crystals
1.2 Crystalline solids
1.3 Crystal symmetry
1.4 Crystal systems
1.5 Miller indices
1.6 Space lattices
1.7 Solid state bonding
1.8 Isomorphs and polymorphs
1.9 Enantiomorphs and chirality
1.10 Crystal habit
1.11 Dendrites
1.12 Composite crystals and twins
1.13 Imperfections in crystals
Chapter 2. Physical and thermal properties
2.1 Density
2.2 Viscosity
2.3 Surface tension
2.4 Diffusivity
2.5 Refractive index
2.6 Electrolytic conductivity
2.7 Crystal hardness
2.8 Units of heat
2.9 Heat capacity
2.10 Thermal conductivity
2.11 Boiling, freezing and melting points
2.12 Enthalpies of phase change
2.13 Heats of solution and crystallization
2.14 Size classification of crystals
Chapter 3. Solutions and solubility
3.1 Solutions and melts
3.2 Solvent selection
3.3 Expression of solution composition
3.4 Solubility correlations
3.5 Theoretical crystal yield
3.6 Ideal and non-ideal solutions
3.7 Particle size and solubility
3.8 Effect of impurities on solubility
3.9 Measurement of solubility
3.10 Prediction of solubility
3.11 Solubility data sources
3.12 Supersolubility
3.13 Solution structure
Chapter 4. Phase equilibria
4.1 The phase rule
4.2 One-component systems
4.3 Two-component systems
4.4 Enthalpy–composition diagrams
4.5 Phase change detection
4.6 Three-component systems
4.7 Four-component systems
4.8 ‘Dynamic’ phase diagrams
Chapter 5. Nucleation
5.1 Primary nucleation
5.2 Secondary nucleation
5.3 Metastable zone widths
5.4 Effect of impurities
5.5 Induction and latent periods
5.6 Interfacial tension
5.7 Ostwald’s rule of stages
Chapter 6. Crystal growth
6.1 Crystal growth theories
6.2 Growth rate measurements
6.3 Crystal growth and dissolution
6.4 Crystal habit modification
6.5 Polymorphs and phase transformations
6.6 Inclusions
Chapter 7. Recrystallization
7.1 Recrystallization schemes
7.2 Resolution of racemates
7.3 Isolation of polymorphs
7.4 Recrystallization from supercritical fluids
7.5 Zone refining
7.6 Single crystals
Chapter 8. Industrial techniques and equipment
8.1 Precipitation
8.2 Crystallization from melts
8.3 Sublimation
8.4 Crystallization from solution
Chapter 9. Crystallizer design and operation
9.1 Crystal size distribution (CSD)
9.2 Kinetic data measurement and utilization
9.3 Crystallizer specification
9.4 Fluid–particle suspensions
9.5 Encrustation
9.6 Caking of crystals
9.7 Downstream processes
Appendix
References
Author index
Subject index
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