Gas chromatography 2nd Edition by Ian Fowlis ISBN 0471954683 9780471954682

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ISBN 10: 0471954683
ISBN 13: 9780471954682
Author: Ian Fowlis

Gas chromatography 2nd Edition Table of contents:

Chapter 1: Introduction to Gas Chromatography

• Overview of Chromatographic Techniques
• History and Development of Gas Chromatography
• Principles of Gas Chromatography
• Components of a Gas Chromatograph: Injector, Column, Detector
• Basic Workflow in Gas Chromatography

Chapter 2: Theory of Gas Chromatography

• The Principles of Separation in GC
• Partition Coefficient and Its Role in GC
• Retention Time and Factors Affecting It
• The Role of the Stationary Phase in GC
• Gas-Liquid Partition Chromatography vs. Gas-Solid Chromatography

Chapter 3: Components of Gas Chromatography

• The Gas Chromatograph Instrument: Detailed Overview
  • Injector: Types and Functions
  • Columns: Capillary vs. Packed Columns
  • Detectors: Flame Ionization Detector (FID), Thermal Conductivity Detector (TCD), Mass Spectrometer (MS), and More
  • Data Acquisition Systems and Software
• Selection of Components Based on Application Needs

Chapter 4: Column Theory and Column Types

• Capillary Columns: Structure, Types, and Applications
• Packed Columns: Characteristics and Uses
• Stationary Phases: Characteristics and Selection
• Column Efficiency and Resolution
• Column Temperature and Pressure: Effects on Separation

Chapter 5: Sample Introduction and Injection Techniques

• Types of Sample Introduction: Liquid, Gas, and Solids
• Split vs. Splitless Injection Techniques
• Sample Preparation: Solvent and Dilution
• Injection Port Design and Optimization

Chapter 6: Detectors in Gas Chromatography

• Overview of GC Detectors: Types and Selection Criteria
• Flame Ionization Detector (FID): Principles and Applications
• Thermal Conductivity Detector (TCD): Working Mechanism and Uses
• Mass Spectrometry (MS) as a Detector in GC
• Other Detectors: Photoionization Detector (PID), Electron Capture Detector (ECD)
• Sensitivity, Linearity, and Detector Performance

Chapter 7: Chromatographic Conditions and Optimization

• Temperature Programming: Techniques and Applications
• Flow Rate Control: Effects on Separation
• Carrier Gas Selection: Helium, Nitrogen, Hydrogen
• Mobile Phase Considerations and Optimization
• Optimizing Retention Time and Resolution

Chapter 8: Quantification and Data Analysis

• Calibration Curves and Quantitative Analysis
• Integration of Chromatographic Peaks
• Sensitivity and Limits of Detection
• Standardization and Quantitative Techniques
• Advanced Data Analysis Techniques: Multivariate Analysis, Chemometrics

Chapter 9: Troubleshooting in Gas Chromatography

• Common Problems in GC: Peak Tailing, Splitting, and Ghost Peaks
• Identifying and Solving Injector, Column, and Detector Issues
• Issues with Sample Preparation and Injection
• Calibration Problems and Solutions
• Preventive Maintenance and Regular Checks

Chapter 10: Applications of Gas Chromatography

• Environmental Analysis: Detection of Pollutants and Contaminants
• Pharmaceutical Analysis: Drug Purity and Dosage Formulation
• Food and Beverage Testing: Flavor, Aroma, and Contaminants
• Forensic Analysis: Blood, Urine, and Other Biological Samples
• Petrochemical and Industrial Applications: Hydrocarbons and Volatile Compounds

Chapter 11: Recent Developments in Gas Chromatography

• Advances in GC Columns: New Materials and Designs
• High-Resolution GC Techniques
• Coupling GC with Mass Spectrometry (GC-MS)
• Miniaturization and Portable GC Systems
• Green Chemistry in Gas Chromatography: Solvent Reduction and Energy Efficiency

Chapter 12: Future Trends in Gas Chromatography

• The Role of Gas Chromatography in Emerging Technologies
• Advances in Automation and High-Throughput GC
• Integration with Other Analytical Techniques
• The Growing Importance of GC in Environmental and Industrial Monitoring
• Innovations in Detectors and Data Processing

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